30 L modular still kit, Liebig condenser

This modular distillation system was created in order to meet the requirements of the most demanding customers. Thanks to the applications of standardising connections and innovative system elements, this system can be used as a basis for configuring various types of stills.

The set includes:

• 340331 - Container - made of stainless steel

Structural characteristics:

- capacity - 30 L

- 2 handles for moving around

- 5 clamping brackets

- cover with a built-in silicone gasket

- installation openings in the cover, intended for thermometer (102700) and still modules

- bottom suitable for gas, electric, and ceramic cooktops.

• 341201 - Still module - 250 mm column connector - made of stainless steel, coming with: silicone gaskets (2 pcs), a complete set of bolts and nuts (4 pcs), and mesh support for the filling (2 pcs).

The connector may perform the function of a catalytic filter, as it enables using a filling that increases the purity of the distillate obtained. The best effect is achieved when using prismatic copper springs. The task of the copper is to adsorb volatile sulphur compounds that provide the distillates with the smell of rotten eggs originating from hydrogen sulphide and have a negative impact on their flavour. The connector can hold about 450 mL of filling, which has to be purchased separately.

Structural characteristics:

- module height - 250 mm.

- external diameter of the module pipe - 48 mm,

- ending with screw connectors

- possibility of using a filling.

• 341202 - Still module - 500 mm column connector - made of stainless steel, coming with: silicone gaskets (2 pcs), a complete set of bolts and nuts (4 pcs), and mesh support for the filling (2 pcs).

The connector may perform the function of a rectifier, as it enables using a filling that increases the purity of the distillate obtained. The best effect is achieved when using prismatic springs or other stainless filling. The connector can hold about 900 ml of filling, which has to be purchased separately.

Structural characteristics:

- module height - 500 mm.

- external diameter of the module pipe - 48 mm

- ending with screw connectors

- possibility of using a filling.

• 341103 - Still module - Reflux - Shotgun - made of stainless steel. Performs the function of an efficient reflux condenser. Comes in a complete set with installation elements: silicone gaskets (2 pcs), a complete set of bolts and nuts (4 pcs), a plug connector, and a throttle check valve. It is intended for precise control of water flow, thanks to which it allows achieving higher degree of distillate purity.

Structural characteristics:

- cooling section height - 100 mm,

- external pipe diameter - 48 mm,

- ending with screw connectors

- two internal passages (shotgun) for distillate vapours, with dimensions of 30/10 mm

- water connection – 2 threaded 1/8” couplers for a hose valve/connector.

• 341005 - Still module - Head - Liebig condenser - made of stainless steel, coming with installation elements: silicone gaskets (2 pcs), a complete set of bolts and nuts (4 pcs), a plug connector + ball valve + stub pipe kit for installing in the condenser. Condenser installed on the top of the distillation column.

Structural characteristics:

- cooling section height - 590 mm

- external pipe diameter - 48 mm

- water connection – threaded 1/8” coupler for a hose valve/connector,

- thermometer (220309) slot.

• 353120 - 5 m soft PVC hose + quick coupling - for connecting cooling water supply to the still.
• 341911 - 10 mm plug connector, Y type - 1 pc.
• Silicone hose for collecting the distillate.
• 102700 - Analog thermometer - for placing inside the container.
• 220309 - Electronic thermometer in a frame - for placing at the connection with the head.

To be purchased separately:

• Stainless steel filling – 1 pack (341901)

• Prismatic copper springs - 1 pack (341900)

• Alcohol meter (405554)

• Proofing parrot (341302).

Description:

Thanks to the shotgun-type dephlegmator it is possible to control the reflux in the column, which has a positive impact on the flavour and aroma of the final product. Thanks to the precise control over the cooling water flow we are capable of not only extracting the appropriate flavours, but also adjusting the concentration of the final product.

Already during the first distillation we can divide the product received into fractions. In this process, the distillate is divided into three fractions: heads (in the amount of about 200 mL), main distillate, and tails.

This division is usually carried out in reference to the temperature in which individual fractions are received, and also to their concentration.

During the course of the process, the temperature rises parabolically while the distillate strength decreases.

The distillate received should be cold. Meanwhile, the temperature of the cooling water in the outflow should be about 60-70°C.

The temperature during the distillation process is adjusted by means of a heat source (e.g. a gas cooker) and the rate of flow of cooling water through the condenser.

Please note: The distillation process should be carried out under supervision.

Kit height without thermometer: about 123 cm

Consumption of cooling water: about 23 L per 1 hour.

Distillation time: 1 hour per 1 L.

CAUTION!

Every country has its own legal regulations governing the manufacturing of ethyl alcohol, wine products, and spirits, introducing them onto the market, and regarding sanctions for non-compliance.